Enantioselective organocatalytic thiol addition to alpha,beta-unsaturated alpha-amino acid derivatives

Authors
Publication date 2012
Journal Synlett
Volume | Issue number 23 | 15
Pages (from-to) 2195-2200
Organisations
  • Faculty of Science (FNWI) - Van 't Hoff Institute for Molecular Sciences (HIMS)
Abstract A new class of Michael acceptors based on α,β-unsaturated amino acids has been prepared and applied in asymmetric ­organocatalysis. With the use of thiourea derivatives of cinchona alkaloid-derived catalysts, efficient addition of thiols to the ­dehydroamino acids occurred with formation of β-thiol functionalized α-amino acids in high yields, moderate diastereoselectivities and ee values up to 95%.

Document type Article
Language English
Published at https://doi.org/10.1055/s-0032-1317081
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